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1H NMR Shift Data for Common Impurities

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Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
residual solvent4.797.267.097.163.312.503.585.321.942.057.145.02
  7.01   1.72   6.993.88
  6.97       6.96 
  2.08         
H2OOH 1.560.430.404.873.332.461.522.132.841.03 
HODOH            
allyl acetateCHCH2  5.935.675.68 5.915.905.92  5.775.93
allyl acetateCHCH2(1)  5.325.055.06 5.295.275.31  5.155.32
allyl acetateCHCH2(2)  5.244.944.94 5.205.155.22  5.045.25
allyl acetateCH2  4.574.344.384.564.524.504.55  4.444.58
allyl acetateCH3  2.091.631.632.052.031.982.05  1.802.07
benzaldehydeHCO  10.039.579.6410.0010.029.9810.01  9.779.88
benzaldehydeCH(2,6)  7.907.467.517.927.927.877.88 7.937.607.91
benzaldehydeCH(3,5)  7.546.976.967.587.647.537.55 7.617.177.58
benzaldehydeCH(4)  7.637.057.047.687.727.627.65 7.717.267.70
benzeneCH  7.367.127.157.337.377.317.357.377.367.207.36
tert-butanolOH  0.581.55 4.193.16 2.18 1.302.20
tert-butyl methyl etherOCH33.22  3.043.20   3.13   
BHAArH  6.766.836.936.716.626.686.73 6.726.836.87
BHAOH 4.764.454.534.856.525.644.76 5.654.62 
BHAArOCH3  3.773.483.483.723.663.683.73 3.723.613.79
BHAArC(CH3)3  1.441.341.411.411.361.401.42 1.411.371.44
Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
BHTArH  6.986.997.056.926.876.926.976.976.966.977.06
BHTOH 5.014.724.79 6.655.815.005.20 5.50 
BHTArCH3  2.272.232.242.212.182.212.252.222.222.202.24
BHTArC(CH3)3  1.431.361.381.401.361.401.421.391.411.371.43
chloroformCH  7.266.106.157.908.327.897.327.588.026.747.33
18-crown-6CH2  3.673.363.393.643.513.573.59 3.593.413.64
cyclohexaneCH2  1.431.401.401.451.401.441.441.441.431.371.47
cyclohexanoneCH2(2,6)  2.331.951.982.342.252.242.29 2.272.082.38
cyclohexanoneCH2(3,5)  1.851.361.331.861.761.801.84 1.811.511.90
cyclohexanoneCH2(4)  1.721.181.121.751.651.701.71 1.721.351.77
diallyl carbonateCHCH2  5.945.635.655.945.935.925.95 5.965.755.92
diallyl carbonateCHCH2(1)  5.375.095.095.345.335.315.35 5.355.175.35
diallyl carbonateCHCH2(2)  5.274.924.925.255.255.195.26 5.235.035.28
diallyl carbonateCH2  4.644.344.384.614.614.584.61 4.624.464.62
1,2-dichloroethaneCH2  3.732.912.903.783.903.773.763.813.873.263.71
dichloromethaneCH2  5.304.324.275.495.765.515.335.445.634.775.24
diglymeCH2 3.673.653.433.463.613.513.433.573.533.563.493.67
dimethyl carbonateCH3  3.793.313.303.743.693.693.75 3.723.483.77
dimethyl malonateCH3  3.753.243.233.723.653.653.72 3.683.413.76
dimethyl malonateCH2  3.402.922.973.443.533.353.37 3.423.153.41
pyridineCH(2,6) 8.528.628.478.538.538.588.548.598.578.588.518.45
dimethylformamideCH 7.928.027.577.637.977.957.917.967.927.967.737.86
pyridineCH(4) 7.877.686.996.987.857.797.657.687.737.767.257.82
pyridineCH(3,5) 7.457.296.676.667.447.397.257.287.337.356.907.40
Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
nitromethaneCH3 4.404.333.012.944.344.424.314.314.314.433.594.28
ethyl acetateCH2CH34.144.123.873.894.094.034.044.084.064.053.964.14
2-propanolCH4.024.043.653.673.923.783.823.973.873.903.824.05
1,4-dioxaneCH2 3.753.713.333.353.663.573.563.653.603.593.453.76
tetrahydrofuranCH2(2,5) 3.743.763.543.573.713.603.623.693.643.633.593.78
ethanolCH23.653.723.363.343.603.443.513.663.543.573.513.71
ethylene glycolCH23.653.763.363.413.593.343.483.663.513.283.583.72
diglymeCH2 3.613.573.313.343.583.383.533.503.453.473.373.62
1,2-dimethoxyethaneCH2 3.603.553.313.333.523.433.433.493.453.463.373.61
diethyl etherCH23.563.483.253.263.493.383.383.433.423.413.313.58
diglymeOCH3 3.373.393.123.113.353.243.283.333.293.283.163.41
1,2-dimethoxyethaneCH3 3.373.403.123.123.353.243.283.343.283.283.173.40
methanolCH33.343.493.033.073.343.163.273.423.283.313.253.44
ethyl methyl ketoneCH2CH33.182.461.821.812.502.432.392.432.432.452.062.49
dimethylacetamideNCH3 3.063.022.562.573.312.942.952.972.963.002.653.05
dimethylformamideCH3 3.012.962.372.362.992.892.882.912.892.942.512.98
dimethylacetamideNCH3 2.902.942.112.052.922.782.822.872.832.832.422.94
dimethylformamideCH3 2.852.881.961.862.862.732.762.822.772.782.302.88
dimethyl sulfoxideCH3 2.712.621.641.682.652.542.452.552.502.522.032.63
HMPACH32.612.652.422.402.642.532.582.602.572.592.472.63
acetoneCH3 2.222.171.571.552.152.092.052.122.08 1.77 
ethyl methyl ketoneCH3CO 2.192.141.591.582.122.072.032.092.062.071.782.16
acetic acidCH32.082.101.571.551.991.911.892.061.961.961.76 
Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
dimethylacetamideCH3CO 2.082.091.591.602.071.961.942.021.971.971.742.09
ethyl acetateCH3CO2.072.051.691.652.011.991.942.001.971.971.782.03
acetonitrileCH3 2.062.100.691.552.03 1.951.971.96   
ethyl methyl ketoneCH2CH31.261.060.840.851.010.910.961.000.960.960.891.05
tert-butanolCH3 1.241.281.031.051.401.111.151.241.161.181.121.28
ethyl acetateCH2CH31.241.260.940.921.241.171.191.231.201.201.041.26
tert-butyl methyl etherCCH31.21  1.071.15   1.14   
diethyl etherCH31.171.211.101.111.181.091.121.151.121.111.101.20
ethaneCH3  0.870.810.800.850.820.850.85 0.830.790.85
ethanolCH31.171.250.970.961.191.061.101.191.121.121.061.22
ethanolOH 1.320.830.50 4.633.301.332.473.391.39 
ethyleneCH2  5.405.255.255.395.415.365.40 5.385.295.40
furanCH(2,5) 7.457.107.137.497.677.487.46 7.567.247.44
furanCH(3,4) 6.406.076.086.406.476.376.41 6.436.196.42
H greaseCH3  0.860.930.940.900.850.880.87 0.900.890.91
H greaseCH2  1.251.331.321.291.241.291.27 1.291.301.33
grease (general)   0.920.88   0.86   
grease (general)   1.361.29   1.27   
hexamethylbenzeneCH3  2.242.102.132.192.142.182.20 2.172.102.24
hexamethyldisiloxaneCH3  0.070.100.120.070.060.070.07 0.070.100.08
n-hexaneCH3 0.880.880.890.900.860.890.890.890.880.850.91
n-hexaneCH2  1.261.221.241.291.251.291.271.281.281.191.31
hydrogenH 4.624.504.474.564.614.554.59 4.544.494.53
Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
imidazoleCH(2)  7.677.307.337.677.637.487.63 7.627.537.61
imidazoleCH(4,5)  7.106.866.907.057.016.947.07 7.047.017.03
methaneCH4  0.220.170.160.200.200.190.21 0.170.150.18
methanolOH 1.09   4.013.021.092.163.121.30 
n-pentaneCH3 0.880.870.870.900.860.890.890.890.880.840.90
n-pentaneCH2  1.271.251.231.291.271.311.301.291.271.231.33
propaneCH3 0.900.890.860.910.870.900.90 0.880.840.90
propaneCH2 1.321.321.261.341.291.331.32 1.311.261.33
2-propanolCH31.171.220.950.951.501.041.081.171.091.101.041.20
propyleneCH3 1.731.551.551.701.681.691.71 1.681.581.70
propyleneCH2(1) 4.944.924.954.914.944.894.93 4.904.914.93
propyleneCH2(2) 5.034.985.015.015.034.995.03 5.004.985.03
propyleneCH  5.835.705.725.825.805.795.84 5.815.725.87
pump oilCH3  0.860.920.940.890.740.880.87 0.870.900.99
pump oilCH2  1.261.301.371.291.151.291.27 1.291.311.41
pyrroleNH  8.407.717.80 10.759.968.69 10.028.61 
pyrroleCH(2,5)  6.836.436.486.726.736.666.79 6.776.626.84
pyrroleCH(3,4)  6.266.276.376.086.016.026.19 6.076.276.24
pyrrolidineCH2(2,5)  2.872.542.542.802.672.752.82  2.643.11
pyrrolidineCH2(3,4)  1.681.361.331.721.551.591.67  1.431.93
silicone greaseCH3  0.070.260.290.10-0.060.110.090.080.130.140.16
tetrahydrofuranCH2(3,4) 1.881.851.431.401.871.761.791.821.801.791.551.91
tolueneCH3 2.362.112.112.322.302.312.342.332.322.162.33
tolueneCH(2,4,6) 7.176.997.027.167.187.107.157.207.157.057.20
tolueneCH(3,5) 7.257.097.137.167.257.197.247.207.157.147.20
Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
triethylamineCH22.572.532.392.402.582.432.462.482.452.452.393.12
triethylamineCH30.991.030.950.961.050.930.970.990.960.960.931.31
Name D2OCDCl3toluene‑d8C6D6CD3ODDMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3