Alistair Boyer

Alistair Boyer

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1H NMR Shift Data for Common Impurities

Switch to 13C.
Click on the solvent name to sort by that solvent. Click on "name" to sort alphabetically.

Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3
residual solvent2.057.267.097.163.314.792.503.585.321.947.145.02
7.011.726.993.88
6.976.96
2.08
pyrroleNH 10.028.407.717.8010.759.968.698.61
pyridineCH(2,6) 8.588.628.478.538.538.528.588.548.598.578.518.45
chloroformCH 8.027.266.106.157.908.327.897.327.586.747.33
dimethylformamideCH 7.968.027.577.637.977.927.957.917.967.927.737.86
benzaldehydeCH(2,6) 7.937.907.467.517.927.927.877.887.607.91
pyridineCH(4) 7.767.686.996.987.857.877.797.657.687.737.257.82
benzaldehydeCH(4) 7.717.637.057.047.687.727.627.657.267.70
imidazoleCH(2) 7.627.677.307.337.677.637.487.637.537.61
benzaldehydeCH(3,5) 7.617.546.976.967.587.647.537.557.177.58
furanCH(2,5)7.567.457.107.137.497.677.487.467.247.44
benzeneCH 7.367.367.127.157.337.377.317.357.377.207.36
pyridineCH(3,5) 7.357.296.676.667.447.457.397.257.287.336.907.40
tolueneCH(2,4,6)7.157.176.997.027.167.187.107.157.207.057.20
tolueneCH(3,5)7.157.257.097.137.167.257.197.247.207.147.20
imidazoleCH(4,5) 7.047.106.866.907.057.016.947.077.017.03
BHTArH 6.966.986.997.056.926.876.926.976.976.977.06
pyrroleCH(2,5) 6.776.836.436.486.726.736.666.796.626.84
BHAArH 6.726.766.836.936.716.626.686.736.836.87
Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3
furanCH(3,4)6.436.406.076.086.406.476.376.416.196.42
pyrroleCH(3,4) 6.076.266.276.376.086.016.026.196.276.24
diallyl carbonateCHCH2 5.965.945.635.655.945.935.925.955.755.92
propyleneCH 5.815.835.705.725.825.805.795.845.725.87
BHAOH5.654.764.454.534.856.525.644.764.62
dichloromethaneCH2 5.635.304.324.275.495.765.515.335.444.775.24
ethyleneCH2 5.385.405.255.255.395.415.365.405.295.40
diallyl carbonateCHCH2(1) 5.355.375.095.095.345.335.315.355.175.35
diallyl carbonateCHCH2(2) 5.235.274.924.925.255.255.195.265.035.28
propyleneCH2(2)5.005.034.985.015.015.034.995.034.985.03
propyleneCH2(1)4.904.944.924.954.914.944.894.934.914.93
diallyl carbonateCH2 4.624.644.344.384.614.614.584.614.464.62
hydrogenH4.544.624.504.474.564.614.554.594.494.53
nitromethaneCH3 4.434.333.012.944.344.404.424.314.314.313.594.28
ethyl acetateCH2CH34.054.123.873.894.094.144.034.044.084.063.964.14
2-propanolCH3.904.043.653.673.924.023.783.823.973.873.824.05
1,2-dichloroethaneCH2 3.873.732.912.903.783.903.773.763.813.263.71
dimethyl carbonateCH3 3.723.793.313.303.743.693.693.753.483.77
BHAArOCH3 3.723.773.483.483.723.663.683.733.613.79
dimethyl malonateCH3 3.683.753.243.233.723.653.653.723.413.76
tetrahydrofuranCH2(2,5) 3.633.763.543.573.713.743.603.623.693.643.593.78
18-crown-6CH2 3.593.673.363.393.643.513.573.593.413.64
1,4-dioxaneCH2 3.593.713.333.353.663.753.573.563.653.603.453.76
Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3
ethanolCH23.573.723.363.343.603.653.443.513.663.543.513.71
diglymeCH2 3.563.653.433.463.613.673.513.433.573.533.493.67
diglymeCH2 3.473.573.313.343.583.613.383.533.503.453.373.62
1,2-dimethoxyethaneCH2 3.463.553.313.333.523.603.433.433.493.453.373.61
dimethyl malonateCH2 3.423.402.922.973.443.533.353.373.153.41
diethyl etherCH23.413.483.253.263.493.563.383.383.433.423.313.58
ethanolOH3.391.320.830.504.633.301.332.471.39
methanolCH33.313.493.033.073.343.343.163.273.423.283.253.44
ethylene glycolCH23.283.763.363.413.593.653.343.483.663.513.583.72
diglymeOCH3 3.283.393.123.113.353.373.243.283.333.293.163.41
1,2-dimethoxyethaneCH3 3.283.403.123.123.353.373.243.283.343.283.173.40
methanolOH3.121.094.013.021.092.161.30
dimethylacetamideNCH3 3.003.022.562.573.313.062.942.952.972.962.653.05
dimethylformamideCH3 2.942.962.372.362.993.012.892.882.912.892.512.98
H2OOH2.841.560.430.404.873.332.461.522.131.03
dimethylacetamideNCH3 2.832.942.112.052.922.902.782.822.872.832.422.94
dimethylformamideCH3 2.782.881.961.862.862.852.732.762.822.772.302.88
HMPACH32.592.652.422.402.642.612.532.582.602.572.472.63
dimethyl sulfoxideCH3 2.522.621.641.682.652.712.542.452.552.502.032.63
ethyl methyl ketoneCH2CH32.452.461.821.812.503.182.432.392.432.432.062.49
triethylamineCH22.452.532.392.402.582.572.432.462.482.452.393.12
tolueneCH32.322.362.112.112.322.302.312.342.332.162.33
cyclohexanoneCH2(2,6) 2.272.331.951.982.342.252.242.292.082.38
Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3
BHTArCH3 2.222.272.232.242.212.182.212.252.222.202.24
hexamethylbenzeneCH3 2.172.242.102.132.192.142.182.202.102.24
ethyl methyl ketoneCH3CO 2.072.141.591.582.122.192.072.032.092.061.782.16
ethyl acetateCH3CO1.972.051.691.652.012.071.991.942.001.971.782.03
dimethylacetamideCH3CO 1.972.091.591.602.072.081.961.942.021.971.742.09
acetic acidCH31.962.101.571.551.992.081.911.892.061.961.76
cyclohexanoneCH2(3,5) 1.811.851.361.331.861.761.801.841.511.90
tetrahydrofuranCH2(3,4) 1.791.851.431.401.871.881.761.791.821.801.551.91
cyclohexanoneCH2(4) 1.721.721.181.121.751.651.701.711.351.77
propyleneCH31.681.731.551.551.701.681.691.711.581.70
cyclohexaneCH2 1.431.431.401.401.451.401.441.441.441.371.47
BHTArC(CH3)3 1.411.431.361.381.401.361.401.421.391.371.43
BHAArC(CH3)3 1.411.441.341.411.411.361.401.421.371.44
propaneCH21.311.321.321.261.341.291.331.321.261.33
H greaseCH2 1.291.251.331.321.291.241.291.271.301.33
pump oilCH2 1.291.261.301.371.291.151.291.271.311.41
n-hexaneCH2 1.281.261.221.241.291.251.291.271.281.191.31
n-pentaneCH2 1.271.271.251.231.291.271.311.301.291.231.33
ethyl acetateCH2CH31.201.260.940.921.241.241.171.191.231.201.041.26
tert-butanolCH3 1.181.281.031.051.401.241.111.151.241.161.121.28
ethanolCH31.121.250.970.961.191.171.061.101.191.121.061.22
diethyl etherCH31.111.211.101.111.181.171.091.121.151.121.101.20
2-propanolCH31.101.220.950.951.501.171.041.081.171.091.041.20
Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3
ethyl methyl ketoneCH2CH30.961.060.840.851.011.260.910.961.000.960.891.05
triethylamineCH30.961.030.950.961.050.990.930.970.990.960.931.31
H greaseCH3 0.900.860.930.940.900.850.880.870.890.91
n-pentaneCH30.880.880.870.870.900.860.890.890.890.840.90
propaneCH30.880.900.890.860.910.870.900.900.840.90
n-hexaneCH30.880.880.880.890.900.860.890.890.890.850.91
pump oilCH3 0.870.860.920.940.890.740.880.870.900.99
ethaneCH3 0.830.870.810.800.850.820.850.850.790.85
methaneCH4 0.170.220.170.160.200.200.190.210.150.18
silicone greaseCH3 0.130.070.260.290.10-0.060.110.090.080.140.16
hexamethyldisiloxaneCH3 0.070.070.100.120.070.060.070.070.100.08
pyrrolidineCH2(3,4) 1.681.361.331.721.551.591.671.431.93
grease (general)1.361.291.27
grease (general)0.920.880.86
pyrrolidineCH2(2,5) 2.872.542.542.802.672.752.822.643.11
HODOH
acetoneCH3 2.171.571.552.152.222.092.052.122.081.77
allyl acetateCHCH2(1) 5.325.055.065.295.275.315.155.32
BHTOH5.014.724.796.655.815.005.205.50
tert-butanolOH0.581.554.193.162.181.302.20
tert-butyl methyl etherOCH33.043.203.223.13
tert-butyl methyl etherCCH31.071.151.211.14
benzaldehydeHCO 10.039.579.6410.0010.029.9810.019.779.88
Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3
allyl acetateCH3 2.091.631.632.052.031.982.051.802.07
allyl acetateCHCH2 5.935.675.685.915.905.925.775.93
allyl acetateCHCH2(2) 5.244.944.945.205.155.225.045.25
allyl acetateCH2 4.574.344.384.564.524.504.554.444.58
acetonitrileCH3 2.100.691.552.032.061.951.971.96
Name acetone‑d6CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNC6D5ClTFE‑d3

alistair@boyer-research.com

School of Chemistry
Joseph Black Building
University of Glasgow
Glasgow, G12 8QQ, UK


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