Alistair Boyer

Alistair Boyer

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1H NMR Shift Data for Common Impurities

Switch to 13C.
Click on the solvent name to sort by that solvent. Click on "name" to sort alphabetically.

Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
residual solvent3.317.267.097.164.792.503.585.321.942.057.145.02
7.011.726.993.88
6.976.96
2.08
benzaldehydeHCO 10.0010.039.579.6410.029.9810.019.779.88
pyridineCH(2,6) 8.538.628.478.538.528.588.548.598.578.588.518.45
dimethylformamideCH 7.978.027.577.637.927.957.917.967.927.967.737.86
benzaldehydeCH(2,6) 7.927.907.467.517.927.877.887.937.607.91
chloroformCH 7.907.266.106.158.327.897.327.588.026.747.33
pyridineCH(4) 7.857.686.996.987.877.797.657.687.737.767.257.82
benzaldehydeCH(4) 7.687.637.057.047.727.627.657.717.267.70
imidazoleCH(2) 7.677.677.307.337.637.487.637.627.537.61
benzaldehydeCH(3,5) 7.587.546.976.967.647.537.557.617.177.58
furanCH(2,5)7.497.457.107.137.677.487.467.567.247.44
pyridineCH(3,5) 7.447.296.676.667.457.397.257.287.337.356.907.40
benzeneCH 7.337.367.127.157.377.317.357.377.367.207.36
tolueneCH(2,4,6)7.167.176.997.027.187.107.157.207.157.057.20
tolueneCH(3,5)7.167.257.097.137.257.197.247.207.157.147.20
imidazoleCH(4,5) 7.057.106.866.907.016.947.077.047.017.03
BHTArH 6.926.986.997.056.876.926.976.976.966.977.06
pyrroleCH(2,5) 6.726.836.436.486.736.666.796.776.626.84
BHAArH 6.716.766.836.936.626.686.736.726.836.87
Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
furanCH(3,4)6.406.406.076.086.476.376.416.436.196.42
pyrroleCH(3,4) 6.086.266.276.376.016.026.196.076.276.24
diallyl carbonateCHCH2 5.945.945.635.655.935.925.955.965.755.92
propyleneCH 5.825.835.705.725.805.795.845.815.725.87
dichloromethaneCH2 5.495.304.324.275.765.515.335.445.634.775.24
ethyleneCH2 5.395.405.255.255.415.365.405.385.295.40
diallyl carbonateCHCH2(1) 5.345.375.095.095.335.315.355.355.175.35
diallyl carbonateCHCH2(2) 5.255.274.924.925.255.195.265.235.035.28
propyleneCH2(2)5.015.034.985.015.034.995.035.004.985.03
propyleneCH2(1)4.914.944.924.954.944.894.934.904.914.93
H2OOH4.871.560.430.403.332.461.522.132.841.03
BHAOH4.854.764.454.536.525.644.765.654.62
diallyl carbonateCH2 4.614.644.344.384.614.584.614.624.464.62
hydrogenH4.564.624.504.474.614.554.594.544.494.53
allyl acetateCH2 4.564.574.344.384.524.504.554.444.58
nitromethaneCH3 4.344.333.012.944.404.424.314.314.314.433.594.28
ethyl acetateCH2CH34.094.123.873.894.144.034.044.084.064.053.964.14
2-propanolCH3.924.043.653.674.023.783.823.973.873.903.824.05
1,2-dichloroethaneCH2 3.783.732.912.903.903.773.763.813.873.263.71
dimethyl carbonateCH3 3.743.793.313.303.693.693.753.723.483.77
dimethyl malonateCH3 3.723.753.243.233.653.653.723.683.413.76
BHAArOCH3 3.723.773.483.483.663.683.733.723.613.79
tetrahydrofuranCH2(2,5) 3.713.763.543.573.743.603.623.693.643.633.593.78
Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
1,4-dioxaneCH2 3.663.713.333.353.753.573.563.653.603.593.453.76
18-crown-6CH2 3.643.673.363.393.513.573.593.593.413.64
diglymeCH2 3.613.653.433.463.673.513.433.573.533.563.493.67
ethanolCH23.603.723.363.343.653.443.513.663.543.573.513.71
ethylene glycolCH23.593.763.363.413.653.343.483.663.513.283.583.72
diglymeCH2 3.583.573.313.343.613.383.533.503.453.473.373.62
1,2-dimethoxyethaneCH2 3.523.553.313.333.603.433.433.493.453.463.373.61
diethyl etherCH23.493.483.253.263.563.383.383.433.423.413.313.58
dimethyl malonateCH2 3.443.402.922.973.533.353.373.423.153.41
1,2-dimethoxyethaneCH3 3.353.403.123.123.373.243.283.343.283.283.173.40
diglymeOCH3 3.353.393.123.113.373.243.283.333.293.283.163.41
methanolCH33.343.493.033.073.343.163.273.423.283.313.253.44
dimethylacetamideNCH3 3.313.022.562.573.062.942.952.972.963.002.653.05
tert-butyl methyl etherOCH33.203.043.223.13
dimethylformamideCH3 2.992.962.372.363.012.892.882.912.892.942.512.98
dimethylacetamideNCH3 2.922.942.112.052.902.782.822.872.832.832.422.94
dimethylformamideCH3 2.862.881.961.862.852.732.762.822.772.782.302.88
pyrrolidineCH2(2,5) 2.802.872.542.542.672.752.822.643.11
dimethyl sulfoxideCH3 2.652.621.641.682.712.542.452.552.502.522.032.63
HMPACH32.642.652.422.402.612.532.582.602.572.592.472.63
triethylamineCH22.582.532.392.402.572.432.462.482.452.452.393.12
ethyl methyl ketoneCH2CH32.502.461.821.813.182.432.392.432.432.452.062.49
cyclohexanoneCH2(2,6) 2.342.331.951.982.252.242.292.272.082.38
Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
tolueneCH32.322.362.112.112.302.312.342.332.322.162.33
BHTArCH3 2.212.272.232.242.182.212.252.222.222.202.24
hexamethylbenzeneCH3 2.192.242.102.132.142.182.202.172.102.24
acetoneCH3 2.152.171.571.552.222.092.052.122.081.77
ethyl methyl ketoneCH3CO 2.122.141.591.582.192.072.032.092.062.071.782.16
dimethylacetamideCH3CO 2.072.091.591.602.081.961.942.021.971.971.742.09
allyl acetateCH3 2.052.091.631.632.031.982.051.802.07
acetonitrileCH3 2.032.100.691.552.061.951.971.96
ethyl acetateCH3CO2.012.051.691.652.071.991.942.001.971.971.782.03
acetic acidCH31.992.101.571.552.081.911.892.061.961.961.76
tetrahydrofuranCH2(3,4) 1.871.851.431.401.881.761.791.821.801.791.551.91
cyclohexanoneCH2(3,5) 1.861.851.361.331.761.801.841.811.511.90
cyclohexanoneCH2(4) 1.751.721.181.121.651.701.711.721.351.77
pyrrolidineCH2(3,4) 1.721.681.361.331.551.591.671.431.93
propyleneCH31.701.731.551.551.681.691.711.681.581.70
2-propanolCH31.501.220.950.951.171.041.081.171.091.101.041.20
cyclohexaneCH2 1.451.431.401.401.401.441.441.441.431.371.47
BHAArC(CH3)3 1.411.441.341.411.361.401.421.411.371.44
tert-butanolCH3 1.401.281.031.051.241.111.151.241.161.181.121.28
BHTArC(CH3)3 1.401.431.361.381.361.401.421.391.411.371.43
propaneCH21.341.321.321.261.291.331.321.311.261.33
n-pentaneCH2 1.291.271.251.231.271.311.301.291.271.231.33
n-hexaneCH2 1.291.261.221.241.251.291.271.281.281.191.31
Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
pump oilCH2 1.291.261.301.371.151.291.271.291.311.41
H greaseCH2 1.291.251.331.321.241.291.271.291.301.33
grease (general)1.291.361.27
ethyl acetateCH2CH31.241.260.940.921.241.171.191.231.201.201.041.26
ethanolCH31.191.250.970.961.171.061.101.191.121.121.061.22
diethyl etherCH31.181.211.101.111.171.091.121.151.121.111.101.20
tert-butyl methyl etherCCH31.151.071.211.14
triethylamineCH31.051.030.950.960.990.930.970.990.960.960.931.31
ethyl methyl ketoneCH2CH31.011.060.840.851.260.910.961.000.960.960.891.05
propaneCH30.910.900.890.860.870.900.900.880.840.90
n-pentaneCH30.900.880.870.870.860.890.890.890.880.840.90
n-hexaneCH30.900.880.880.890.860.890.890.890.880.850.91
H greaseCH3 0.900.860.930.940.850.880.870.900.890.91
pump oilCH3 0.890.860.920.940.740.880.870.870.900.99
grease (general)0.880.920.86
ethaneCH3 0.850.870.810.800.820.850.850.830.790.85
methaneCH4 0.200.220.170.160.200.190.210.170.150.18
silicone greaseCH3 0.100.070.260.29-0.060.110.090.080.130.140.16
hexamethyldisiloxaneCH3 0.070.070.100.120.060.070.070.070.100.08
HODOH
methanolOH1.094.013.021.092.163.121.30
BHTOH5.014.724.796.655.815.005.205.50
tert-butanolOH0.581.554.193.162.181.302.20
Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
allyl acetateCHCH2(2) 5.244.944.945.205.155.225.045.25
pyrroleNH 8.407.717.8010.759.968.6910.028.61
allyl acetateCHCH2 5.935.675.685.915.905.925.775.93
allyl acetateCHCH2(1) 5.325.055.065.295.275.315.155.32
ethanolOH1.320.830.504.633.301.332.473.391.39
Name CD3ODCDCl3toluene‑d8C6D6D2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3

alistair@boyer-research.com

School of Chemistry
Joseph Black Building
University of Glasgow
Glasgow, G12 8QQ, UK


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