Alistair Boyer

Alistair Boyer

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1H NMR Shift Data for Common Impurities

Switch to 13C.
Click on the solvent name to sort by that solvent. Click on "name" to sort alphabetically.

Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3
residual solvent5.327.267.097.163.314.792.503.581.942.057.145.02
7.011.726.993.88
6.976.96
2.08
benzaldehydeHCO 10.0110.039.579.6410.0010.029.989.779.88
pyrroleNH 8.698.407.717.8010.759.9610.028.61
pyridineCH(2,6) 8.598.628.478.538.538.528.588.548.578.588.518.45
dimethylformamideCH 7.968.027.577.637.977.927.957.917.927.967.737.86
benzaldehydeCH(2,6) 7.887.907.467.517.927.927.877.937.607.91
pyridineCH(4) 7.687.686.996.987.857.877.797.657.737.767.257.82
benzaldehydeCH(4) 7.657.637.057.047.687.727.627.717.267.70
imidazoleCH(2) 7.637.677.307.337.677.637.487.627.537.61
benzaldehydeCH(3,5) 7.557.546.976.967.587.647.537.617.177.58
furanCH(2,5)7.467.457.107.137.497.677.487.567.247.44
benzeneCH 7.357.367.127.157.337.377.317.377.367.207.36
chloroformCH 7.327.266.106.157.908.327.897.588.026.747.33
pyridineCH(3,5) 7.287.296.676.667.447.457.397.257.337.356.907.40
tolueneCH(3,5)7.247.257.097.137.167.257.197.207.157.147.20
tolueneCH(2,4,6)7.157.176.997.027.167.187.107.207.157.057.20
imidazoleCH(4,5) 7.077.106.866.907.057.016.947.047.017.03
BHTArH 6.976.986.997.056.926.876.926.976.966.977.06
pyrroleCH(2,5) 6.796.836.436.486.726.736.666.776.626.84
Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3
BHAArH 6.736.766.836.936.716.626.686.726.836.87
furanCH(3,4)6.416.406.076.086.406.476.376.436.196.42
pyrroleCH(3,4) 6.196.266.276.376.086.016.026.076.276.24
diallyl carbonateCHCH2 5.955.945.635.655.945.935.925.965.755.92
allyl acetateCHCH2 5.925.935.675.685.915.905.775.93
propyleneCH 5.845.835.705.725.825.805.795.815.725.87
ethyleneCH2 5.405.405.255.255.395.415.365.385.295.40
diallyl carbonateCHCH2(1) 5.355.375.095.095.345.335.315.355.175.35
dichloromethaneCH2 5.335.304.324.275.495.765.515.445.634.775.24
allyl acetateCHCH2(1) 5.315.325.055.065.295.275.155.32
diallyl carbonateCHCH2(2) 5.265.274.924.925.255.255.195.235.035.28
allyl acetateCHCH2(2) 5.225.244.944.945.205.155.045.25
propyleneCH2(2)5.035.034.985.015.015.034.995.004.985.03
BHTOH5.005.014.724.796.655.815.205.50
propyleneCH2(1)4.934.944.924.954.914.944.894.904.914.93
BHAOH4.764.764.454.534.856.525.645.654.62
diallyl carbonateCH2 4.614.644.344.384.614.614.584.624.464.62
hydrogenH4.594.624.504.474.564.614.554.544.494.53
allyl acetateCH2 4.554.574.344.384.564.524.504.444.58
nitromethaneCH3 4.314.333.012.944.344.404.424.314.314.433.594.28
ethyl acetateCH2CH34.084.123.873.894.094.144.034.044.064.053.964.14
2-propanolCH3.974.043.653.673.924.023.783.823.873.903.824.05
1,2-dichloroethaneCH2 3.763.732.912.903.783.903.773.813.873.263.71
Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3
dimethyl carbonateCH3 3.753.793.313.303.743.693.693.723.483.77
BHAArOCH3 3.733.773.483.483.723.663.683.723.613.79
dimethyl malonateCH3 3.723.753.243.233.723.653.653.683.413.76
tetrahydrofuranCH2(2,5) 3.693.763.543.573.713.743.603.623.643.633.593.78
ethanolCH23.663.723.363.343.603.653.443.513.543.573.513.71
ethylene glycolCH23.663.763.363.413.593.653.343.483.513.283.583.72
1,4-dioxaneCH2 3.653.713.333.353.663.753.573.563.603.593.453.76
18-crown-6CH2 3.593.673.363.393.643.513.573.593.413.64
diglymeCH2 3.573.653.433.463.613.673.513.433.533.563.493.67
diglymeCH2 3.503.573.313.343.583.613.383.533.453.473.373.62
1,2-dimethoxyethaneCH2 3.493.553.313.333.523.603.433.433.453.463.373.61
diethyl etherCH23.433.483.253.263.493.563.383.383.423.413.313.58
methanolCH33.423.493.033.073.343.343.163.273.283.313.253.44
dimethyl malonateCH2 3.373.402.922.973.443.533.353.423.153.41
1,2-dimethoxyethaneCH3 3.343.403.123.123.353.373.243.283.283.283.173.40
diglymeOCH3 3.333.393.123.113.353.373.243.283.293.283.163.41
dimethylacetamideNCH3 2.973.022.562.573.313.062.942.952.963.002.653.05
dimethylformamideCH3 2.912.962.372.362.993.012.892.882.892.942.512.98
dimethylacetamideNCH3 2.872.942.112.052.922.902.782.822.832.832.422.94
pyrrolidineCH2(2,5) 2.822.872.542.542.802.672.752.643.11
dimethylformamideCH3 2.822.881.961.862.862.852.732.762.772.782.302.88
HMPACH32.602.652.422.402.642.612.532.582.572.592.472.63
dimethyl sulfoxideCH3 2.552.621.641.682.652.712.542.452.502.522.032.63
Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3
triethylamineCH22.482.532.392.402.582.572.432.462.452.452.393.12
ethyl methyl ketoneCH2CH32.432.461.821.812.503.182.432.392.432.452.062.49
tolueneCH32.342.362.112.112.322.302.312.332.322.162.33
cyclohexanoneCH2(2,6) 2.292.331.951.982.342.252.242.272.082.38
BHTArCH3 2.252.272.232.242.212.182.212.222.222.202.24
hexamethylbenzeneCH3 2.202.242.102.132.192.142.182.172.102.24
acetoneCH3 2.122.171.571.552.152.222.092.052.081.77
ethyl methyl ketoneCH3CO 2.092.141.591.582.122.192.072.032.062.071.782.16
acetic acidCH32.062.101.571.551.992.081.911.891.961.961.76
allyl acetateCH3 2.052.091.631.632.052.031.981.802.07
dimethylacetamideCH3CO 2.022.091.591.602.072.081.961.941.971.971.742.09
ethyl acetateCH3CO2.002.051.691.652.012.071.991.941.971.971.782.03
acetonitrileCH3 1.972.100.691.552.032.061.951.96
cyclohexanoneCH2(3,5) 1.841.851.361.331.861.761.801.811.511.90
tetrahydrofuranCH2(3,4) 1.821.851.431.401.871.881.761.791.801.791.551.91
propyleneCH31.711.731.551.551.701.681.691.681.581.70
cyclohexanoneCH2(4) 1.711.721.181.121.751.651.701.721.351.77
pyrrolidineCH2(3,4) 1.671.681.361.331.721.551.591.431.93
H2OOH1.521.560.430.404.873.332.462.132.841.03
cyclohexaneCH2 1.441.431.401.401.451.401.441.441.431.371.47
BHAArC(CH3)3 1.421.441.341.411.411.361.401.411.371.44
BHTArC(CH3)3 1.421.431.361.381.401.361.401.391.411.371.43
ethanolOH1.331.320.830.504.633.302.473.391.39
Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3
propaneCH21.321.321.321.261.341.291.331.311.261.33
n-pentaneCH2 1.301.271.251.231.291.271.311.291.271.231.33
n-hexaneCH2 1.271.261.221.241.291.251.291.281.281.191.31
pump oilCH2 1.271.261.301.371.291.151.291.291.311.41
H greaseCH2 1.271.251.331.321.291.241.291.291.301.33
tert-butanolCH3 1.241.281.031.051.401.241.111.151.161.181.121.28
ethyl acetateCH2CH31.231.260.940.921.241.241.171.191.201.201.041.26
ethanolCH31.191.250.970.961.191.171.061.101.121.121.061.22
2-propanolCH31.171.220.950.951.501.171.041.081.091.101.041.20
diethyl etherCH31.151.211.101.111.181.171.091.121.121.111.101.20
methanolOH1.091.094.013.022.163.121.30
ethyl methyl ketoneCH2CH31.001.060.840.851.011.260.910.960.960.960.891.05
triethylamineCH30.991.030.950.961.050.990.930.970.960.960.931.31
propaneCH30.900.900.890.860.910.870.900.880.840.90
n-pentaneCH30.890.880.870.870.900.860.890.890.880.840.90
n-hexaneCH30.890.880.880.890.900.860.890.890.880.850.91
H greaseCH3 0.870.860.930.940.900.850.880.900.890.91
pump oilCH3 0.870.860.920.940.890.740.880.870.900.99
ethaneCH3 0.850.870.810.800.850.820.850.830.790.85
methaneCH4 0.210.220.170.160.200.200.190.170.150.18
silicone greaseCH3 0.090.070.260.290.10-0.060.110.080.130.140.16
hexamethyldisiloxaneCH3 0.070.070.100.120.070.060.070.070.100.08
grease (general)0.920.880.86
Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3
tert-butyl methyl etherCCH31.071.151.211.14
grease (general)1.361.291.27
HODOH
tert-butyl methyl etherOCH33.043.203.223.13
tert-butanolOH0.581.554.193.162.181.302.20
Name CD2Cl2CDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD3CNacetone‑d6C6D5ClTFE‑d3

alistair@boyer-research.com

School of Chemistry
Joseph Black Building
University of Glasgow
Glasgow, G12 8QQ, UK


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