Alistair Boyer

Alistair Boyer

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1H NMR Shift Data for Common Impurities

Switch to 13C.
Click on the solvent name to sort by that solvent. Click on "name" to sort alphabetically.

Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
residual solvent7.167.267.093.314.792.503.585.321.942.057.145.02
7.011.726.993.88
6.976.96
2.08
benzaldehydeHCO 9.6410.039.5710.0010.029.9810.019.779.88
pyridineCH(2,6) 8.538.628.478.538.528.588.548.598.578.588.518.45
pyrroleNH 7.808.407.7110.759.968.6910.028.61
dimethylformamideCH 7.638.027.577.977.927.957.917.967.927.967.737.86
benzaldehydeCH(2,6) 7.517.907.467.927.927.877.887.937.607.91
imidazoleCH(2) 7.337.677.307.677.637.487.637.627.537.61
benzeneCH 7.157.367.127.337.377.317.357.377.367.207.36
tolueneCH(3,5)7.137.257.097.167.257.197.247.207.157.147.20
furanCH(2,5)7.137.457.107.497.677.487.467.567.247.44
BHTArH 7.056.986.996.926.876.926.976.976.966.977.06
benzaldehydeCH(4) 7.047.637.057.687.727.627.657.717.267.70
tolueneCH(2,4,6)7.027.176.997.167.187.107.157.207.157.057.20
pyridineCH(4) 6.987.686.997.857.877.797.657.687.737.767.257.82
benzaldehydeCH(3,5) 6.967.546.977.587.647.537.557.617.177.58
BHAArH 6.936.766.836.716.626.686.736.726.836.87
imidazoleCH(4,5) 6.907.106.867.057.016.947.077.047.017.03
pyridineCH(3,5) 6.667.296.677.447.457.397.257.287.337.356.907.40
pyrroleCH(2,5) 6.486.836.436.726.736.666.796.776.626.84
pyrroleCH(3,4) 6.376.266.276.086.016.026.196.076.276.24
Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
chloroformCH 6.157.266.107.908.327.897.327.588.026.747.33
furanCH(3,4)6.086.406.076.406.476.376.416.436.196.42
propyleneCH 5.725.835.705.825.805.795.845.815.725.87
allyl acetateCHCH2 5.685.935.675.915.905.925.775.93
diallyl carbonateCHCH2 5.655.945.635.945.935.925.955.965.755.92
ethyleneCH2 5.255.405.255.395.415.365.405.385.295.40
diallyl carbonateCHCH2(1) 5.095.375.095.345.335.315.355.355.175.35
allyl acetateCHCH2(1) 5.065.325.055.295.275.315.155.32
propyleneCH2(2)5.015.034.985.015.034.995.035.004.985.03
propyleneCH2(1)4.954.944.924.914.944.894.934.904.914.93
allyl acetateCHCH2(2) 4.945.244.945.205.155.225.045.25
diallyl carbonateCHCH2(2) 4.925.274.925.255.255.195.265.235.035.28
BHTOH4.795.014.726.655.815.005.205.50
BHAOH4.534.764.454.856.525.644.765.654.62
hydrogenH4.474.624.504.564.614.554.594.544.494.53
allyl acetateCH2 4.384.574.344.564.524.504.554.444.58
diallyl carbonateCH2 4.384.644.344.614.614.584.614.624.464.62
dichloromethaneCH2 4.275.304.325.495.765.515.335.445.634.775.24
ethyl acetateCH2CH33.894.123.874.094.144.034.044.084.064.053.964.14
2-propanolCH3.674.043.653.924.023.783.823.973.873.903.824.05
tetrahydrofuranCH2(2,5) 3.573.763.543.713.743.603.623.693.643.633.593.78
BHAArOCH3 3.483.773.483.723.663.683.733.723.613.79
diglymeCH2 3.463.653.433.613.673.513.433.573.533.563.493.67
Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
ethylene glycolCH23.413.763.363.593.653.343.483.663.513.283.583.72
18-crown-6CH2 3.393.673.363.643.513.573.593.593.413.64
1,4-dioxaneCH2 3.353.713.333.663.753.573.563.653.603.593.453.76
diglymeCH2 3.343.573.313.583.613.383.533.503.453.473.373.62
ethanolCH23.343.723.363.603.653.443.513.663.543.573.513.71
1,2-dimethoxyethaneCH2 3.333.553.313.523.603.433.433.493.453.463.373.61
dimethyl carbonateCH3 3.303.793.313.743.693.693.753.723.483.77
diethyl etherCH23.263.483.253.493.563.383.383.433.423.413.313.58
dimethyl malonateCH3 3.233.753.243.723.653.653.723.683.413.76
1,2-dimethoxyethaneCH3 3.123.403.123.353.373.243.283.343.283.283.173.40
diglymeOCH3 3.113.393.123.353.373.243.283.333.293.283.163.41
methanolCH33.073.493.033.343.343.163.273.423.283.313.253.44
tert-butyl methyl etherOCH33.043.203.223.13
dimethyl malonateCH2 2.973.402.923.443.533.353.373.423.153.41
nitromethaneCH3 2.944.333.014.344.404.424.314.314.314.433.594.28
1,2-dichloroethaneCH2 2.903.732.913.783.903.773.763.813.873.263.71
dimethylacetamideNCH3 2.573.022.563.313.062.942.952.972.963.002.653.05
pyrrolidineCH2(2,5) 2.542.872.542.802.672.752.822.643.11
HMPACH32.402.652.422.642.612.532.582.602.572.592.472.63
triethylamineCH22.402.532.392.582.572.432.462.482.452.452.393.12
dimethylformamideCH3 2.362.962.372.993.012.892.882.912.892.942.512.98
BHTArCH3 2.242.272.232.212.182.212.252.222.222.202.24
hexamethylbenzeneCH3 2.132.242.102.192.142.182.202.172.102.24
Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
tolueneCH32.112.362.112.322.302.312.342.332.322.162.33
dimethylacetamideNCH3 2.052.942.112.922.902.782.822.872.832.832.422.94
cyclohexanoneCH2(2,6) 1.982.331.952.342.252.242.292.272.082.38
dimethylformamideCH3 1.862.881.962.862.852.732.762.822.772.782.302.88
ethyl methyl ketoneCH2CH31.812.461.822.503.182.432.392.432.432.452.062.49
dimethyl sulfoxideCH3 1.682.621.642.652.712.542.452.552.502.522.032.63
ethyl acetateCH3CO1.652.051.692.012.071.991.942.001.971.971.782.03
allyl acetateCH3 1.632.091.632.052.031.982.051.802.07
dimethylacetamideCH3CO 1.602.091.592.072.081.961.942.021.971.971.742.09
ethyl methyl ketoneCH3CO 1.582.141.592.122.192.072.032.092.062.071.782.16
acetonitrileCH3 1.552.100.692.032.061.951.971.96
propyleneCH31.551.731.551.701.681.691.711.681.581.70
tert-butanolOH1.550.584.193.162.181.302.20
acetic acidCH31.552.101.571.992.081.911.892.061.961.961.76
acetoneCH3 1.552.171.572.152.222.092.052.122.081.77
BHAArC(CH3)3 1.411.441.341.411.361.401.421.411.371.44
cyclohexaneCH2 1.401.431.401.451.401.441.441.441.431.371.47
tetrahydrofuranCH2(3,4) 1.401.851.431.871.881.761.791.821.801.791.551.91
BHTArC(CH3)3 1.381.431.361.401.361.401.421.391.411.371.43
pump oilCH2 1.371.261.301.291.151.291.271.291.311.41
grease (general)1.361.291.27
pyrrolidineCH2(3,4) 1.331.681.361.721.551.591.671.431.93
cyclohexanoneCH2(3,5) 1.331.851.361.861.761.801.841.811.511.90
Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
H greaseCH2 1.321.251.331.291.241.291.271.291.301.33
propaneCH21.261.321.321.341.291.331.321.311.261.33
n-hexaneCH2 1.241.261.221.291.251.291.271.281.281.191.31
n-pentaneCH2 1.231.271.251.291.271.311.301.291.271.231.33
cyclohexanoneCH2(4) 1.121.721.181.751.651.701.711.721.351.77
diethyl etherCH31.111.211.101.181.171.091.121.151.121.111.101.20
tert-butyl methyl etherCCH31.071.151.211.14
tert-butanolCH3 1.051.281.031.401.241.111.151.241.161.181.121.28
triethylamineCH30.961.030.951.050.990.930.970.990.960.960.931.31
ethanolCH30.961.250.971.191.171.061.101.191.121.121.061.22
2-propanolCH30.951.220.951.501.171.041.081.171.091.101.041.20
H greaseCH3 0.940.860.930.900.850.880.870.900.890.91
pump oilCH3 0.940.860.920.890.740.880.870.870.900.99
grease (general)0.920.880.86
ethyl acetateCH2CH30.921.260.941.241.241.171.191.231.201.201.041.26
n-hexaneCH30.890.880.880.900.860.890.890.890.880.850.91
n-pentaneCH30.870.880.870.900.860.890.890.890.880.840.90
propaneCH30.860.900.890.910.870.900.900.880.840.90
ethyl methyl ketoneCH2CH30.851.060.841.011.260.910.961.000.960.960.891.05
ethaneCH3 0.800.870.810.850.820.850.850.830.790.85
ethanolOH0.501.320.834.633.301.332.473.391.39
H2OOH0.401.560.434.873.332.461.522.132.841.03
silicone greaseCH3 0.290.070.260.10-0.060.110.090.080.130.140.16
Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3
methaneCH4 0.160.220.170.200.200.190.210.170.150.18
hexamethyldisiloxaneCH3 0.120.070.100.070.060.070.070.070.100.08
methanolOH1.094.013.021.092.163.121.30
HODOH
Name C6D6CDCl3toluene‑d8CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6C6D5ClTFE‑d3

alistair@boyer-research.com

School of Chemistry
Joseph Black Building
University of Glasgow
Glasgow, G12 8QQ, UK


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