Alistair Boyer

Alistair Boyer

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1H NMR Shift Data for Common Impurities

Switch to 13C.
Click on the solvent name to sort by that solvent. Click on "name" to sort alphabetically.

Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3
residual solvent7.147.267.097.163.314.792.503.585.321.942.055.02
6.997.011.723.88
6.966.97
2.08
benzaldehydeHCO 9.7710.039.579.6410.0010.029.9810.019.88
pyrroleNH 8.618.407.717.8010.759.968.6910.02
pyridineCH(2,6) 8.518.628.478.538.538.528.588.548.598.578.588.45
dimethylformamideCH 7.738.027.577.637.977.927.957.917.967.927.967.86
benzaldehydeCH(2,6) 7.607.907.467.517.927.927.877.887.937.91
imidazoleCH(2) 7.537.677.307.337.677.637.487.637.627.61
benzaldehydeCH(4) 7.267.637.057.047.687.727.627.657.717.70
pyridineCH(4) 7.257.686.996.987.857.877.797.657.687.737.767.82
furanCH(2,5)7.247.457.107.137.497.677.487.467.567.44
benzeneCH 7.207.367.127.157.337.377.317.357.377.367.36
benzaldehydeCH(3,5) 7.177.546.976.967.587.647.537.557.617.58
tolueneCH(3,5)7.147.257.097.137.167.257.197.247.207.157.20
tolueneCH(2,4,6)7.057.176.997.027.167.187.107.157.207.157.20
imidazoleCH(4,5) 7.017.106.866.907.057.016.947.077.047.03
BHTArH 6.976.986.997.056.926.876.926.976.976.967.06
pyridineCH(3,5) 6.907.296.676.667.447.457.397.257.287.337.357.40
BHAArH 6.836.766.836.936.716.626.686.736.726.87
chloroformCH 6.747.266.106.157.908.327.897.327.588.027.33
Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3
pyrroleCH(2,5) 6.626.836.436.486.726.736.666.796.776.84
pyrroleCH(3,4) 6.276.266.276.376.086.016.026.196.076.24
furanCH(3,4)6.196.406.076.086.406.476.376.416.436.42
allyl acetateCHCH2 5.775.935.675.685.915.905.925.93
diallyl carbonateCHCH2 5.755.945.635.655.945.935.925.955.965.92
propyleneCH 5.725.835.705.725.825.805.795.845.815.87
BHTOH5.505.014.724.796.655.815.005.20
ethyleneCH2 5.295.405.255.255.395.415.365.405.385.40
diallyl carbonateCHCH2(1) 5.175.375.095.095.345.335.315.355.355.35
allyl acetateCHCH2(1) 5.155.325.055.065.295.275.315.32
allyl acetateCHCH2(2) 5.045.244.944.945.205.155.225.25
diallyl carbonateCHCH2(2) 5.035.274.924.925.255.255.195.265.235.28
propyleneCH2(2)4.985.034.985.015.015.034.995.035.005.03
propyleneCH2(1)4.914.944.924.954.914.944.894.934.904.93
dichloromethaneCH2 4.775.304.324.275.495.765.515.335.445.635.24
BHAOH4.624.764.454.534.856.525.644.765.65
hydrogenH4.494.624.504.474.564.614.554.594.544.53
diallyl carbonateCH2 4.464.644.344.384.614.614.584.614.624.62
allyl acetateCH2 4.444.574.344.384.564.524.504.554.58
ethyl acetateCH2CH33.964.123.873.894.094.144.034.044.084.064.054.14
2-propanolCH3.824.043.653.673.924.023.783.823.973.873.904.05
BHAArOCH3 3.613.773.483.483.723.663.683.733.723.79
nitromethaneCH3 3.594.333.012.944.344.404.424.314.314.314.434.28
Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3
tetrahydrofuranCH2(2,5) 3.593.763.543.573.713.743.603.623.693.643.633.78
ethylene glycolCH23.583.763.363.413.593.653.343.483.663.513.283.72
ethanolCH23.513.723.363.343.603.653.443.513.663.543.573.71
diglymeCH2 3.493.653.433.463.613.673.513.433.573.533.563.67
dimethyl carbonateCH3 3.483.793.313.303.743.693.693.753.723.77
1,4-dioxaneCH2 3.453.713.333.353.663.753.573.563.653.603.593.76
dimethyl malonateCH3 3.413.753.243.233.723.653.653.723.683.76
18-crown-6CH2 3.413.673.363.393.643.513.573.593.593.64
diglymeCH2 3.373.573.313.343.583.613.383.533.503.453.473.62
1,2-dimethoxyethaneCH2 3.373.553.313.333.523.603.433.433.493.453.463.61
diethyl etherCH23.313.483.253.263.493.563.383.383.433.423.413.58
1,2-dichloroethaneCH2 3.263.732.912.903.783.903.773.763.813.873.71
methanolCH33.253.493.033.073.343.343.163.273.423.283.313.44
1,2-dimethoxyethaneCH3 3.173.403.123.123.353.373.243.283.343.283.283.40
diglymeOCH3 3.163.393.123.113.353.373.243.283.333.293.283.41
dimethyl malonateCH2 3.153.402.922.973.443.533.353.373.423.41
dimethylacetamideNCH3 2.653.022.562.573.313.062.942.952.972.963.003.05
pyrrolidineCH2(2,5) 2.642.872.542.542.802.672.752.823.11
dimethylformamideCH3 2.512.962.372.362.993.012.892.882.912.892.942.98
HMPACH32.472.652.422.402.642.612.532.582.602.572.592.63
dimethylacetamideNCH3 2.422.942.112.052.922.902.782.822.872.832.832.94
triethylamineCH22.392.532.392.402.582.572.432.462.482.452.453.12
dimethylformamideCH3 2.302.881.961.862.862.852.732.762.822.772.782.88
Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3
BHTArCH3 2.202.272.232.242.212.182.212.252.222.222.24
tolueneCH32.162.362.112.112.322.302.312.342.332.322.33
hexamethylbenzeneCH3 2.102.242.102.132.192.142.182.202.172.24
cyclohexanoneCH2(2,6) 2.082.331.951.982.342.252.242.292.272.38
ethyl methyl ketoneCH2CH32.062.461.821.812.503.182.432.392.432.432.452.49
dimethyl sulfoxideCH3 2.032.621.641.682.652.712.542.452.552.502.522.63
allyl acetateCH3 1.802.091.631.632.052.031.982.052.07
ethyl acetateCH3CO1.782.051.691.652.012.071.991.942.001.971.972.03
ethyl methyl ketoneCH3CO 1.782.141.591.582.122.192.072.032.092.062.072.16
acetoneCH3 1.772.171.571.552.152.222.092.052.122.08
acetic acidCH31.762.101.571.551.992.081.911.892.061.961.96
dimethylacetamideCH3CO 1.742.091.591.602.072.081.961.942.021.971.972.09
propyleneCH31.581.731.551.551.701.681.691.711.681.70
tetrahydrofuranCH2(3,4) 1.551.851.431.401.871.881.761.791.821.801.791.91
cyclohexanoneCH2(3,5) 1.511.851.361.331.861.761.801.841.811.90
pyrrolidineCH2(3,4) 1.431.681.361.331.721.551.591.671.93
ethanolOH1.391.320.830.504.633.301.332.473.39
BHTArC(CH3)3 1.371.431.361.381.401.361.401.421.391.411.43
BHAArC(CH3)3 1.371.441.341.411.411.361.401.421.411.44
cyclohexaneCH2 1.371.431.401.401.451.401.441.441.441.431.47
cyclohexanoneCH2(4) 1.351.721.181.121.751.651.701.711.721.77
pump oilCH2 1.311.261.301.371.291.151.291.271.291.41
methanolOH1.301.094.013.021.092.163.12
Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3
tert-butanolOH1.300.581.554.193.162.182.20
H greaseCH2 1.301.251.331.321.291.241.291.271.291.33
propaneCH21.261.321.321.261.341.291.331.321.311.33
n-pentaneCH2 1.231.271.251.231.291.271.311.301.291.271.33
n-hexaneCH2 1.191.261.221.241.291.251.291.271.281.281.31
tert-butanolCH3 1.121.281.031.051.401.241.111.151.241.161.181.28
diethyl etherCH31.101.211.101.111.181.171.091.121.151.121.111.20
ethanolCH31.061.250.970.961.191.171.061.101.191.121.121.22
ethyl acetateCH2CH31.041.260.940.921.241.241.171.191.231.201.201.26
2-propanolCH31.041.220.950.951.501.171.041.081.171.091.101.20
H2OOH1.031.560.430.404.873.332.461.522.132.84
triethylamineCH30.931.030.950.961.050.990.930.970.990.960.961.31
pump oilCH3 0.900.860.920.940.890.740.880.870.870.99
ethyl methyl ketoneCH2CH30.891.060.840.851.011.260.910.961.000.960.961.05
H greaseCH3 0.890.860.930.940.900.850.880.870.900.91
n-hexaneCH30.850.880.880.890.900.860.890.890.890.880.91
n-pentaneCH30.840.880.870.870.900.860.890.890.890.880.90
propaneCH30.840.900.890.860.910.870.900.900.880.90
ethaneCH3 0.790.870.810.800.850.820.850.850.830.85
methaneCH4 0.150.220.170.160.200.200.190.210.170.18
silicone greaseCH3 0.140.070.260.290.10-0.060.110.090.080.130.16
hexamethyldisiloxaneCH3 0.100.070.100.120.070.060.070.070.070.08
HODOH
Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3
acetonitrileCH3 2.100.691.552.032.061.951.971.96
tert-butyl methyl etherOCH33.043.203.223.13
tert-butyl methyl etherCCH31.071.151.211.14
grease (general)1.361.291.27
grease (general)0.920.880.86
Name C6D5ClCDCl3toluene‑d8C6D6CD3ODD2ODMSO‑d6THF‑d8CD2Cl2CD3CNacetone‑d6TFE‑d3

alistair@boyer-research.com

School of Chemistry
Joseph Black Building
University of Glasgow
Glasgow, G12 8QQ, UK


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